4-Methyl-N-(9-methyl-9-azabicyclo[3.3.1]non-3-yl)benzamide

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4-Methyl-N-(9-methyl-9-aza­bicyclo­[3.3.1]non-3-yl)benzamide

The asymmetric unit of the title compound, C(17)H(24)N(2)O, contains three independent mol-ecules. In the crystal, mol-ecules are linked by weak N-H⋯O hydrogen bonds into chains parallel to the c axis.

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Diaqua­bis[3-(2-hydroxy­ethyl)-2-methyl-4-oxopyrido[1,2-a]pyrimidin-9-olato-κ2 N 1,O 9]manganese(II)

The title compound, [Mn(C(11)H(11)N(2)O(3))(2)(H(2)O)(2)], consists of discrete mononuclear complex mol-ecules. The Mn(II) atom is located on an inversion center and coordinated by two N atoms and two O atoms, each pair in a trans mode, from two 3-(2-hydroxy-ethyl)-2-methyl-4-oxopyrido[1,2-a]pyrimidin-9-olate ligands and by two water mol-ecules. The coordination geometry around the Mn(II) atom ...

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4-Methyl-N-(3-methyl­phen­yl)benzene­sulfonamide

In the title compound, C(14)H(15)NO(2)S, the conformation of the N-C bond in the C-SO(2)-NH-C segment has gauche torsion angles with respect to the S=O bonds. Further, the conformation of the N-H bond is anti to the 3-methyl group in the aniline benzene ring. The mol-ecule is bent at the N atom with a C-SO(2)-NH-C torsion angle of 56.7 (3)°. The dihedral angle between the benzene rings is 83.9 ...

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(E)-4-Methyl-N′-(3-nitro­benzyl­idene)benzohydrazide

In the title compound, C(15)H(13)N(3)O(3), the dihedral angle between the benzene rings is 1.01 (3)° and that between the nitro group and its attached ring is 5.99 (15)°. In the crystal, mol-ecules are linked by N-H⋯O hydrogen bonds generating C(4) chains along [010].

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3-Methyl-N-(4-methyl­phen­yl)benzamide

In the title compound, C(15)H(15)NO, the two aromatic rings make a dihedral angle of 70.06 (3)°, while the central amide core -NH-C(=O)- is twisted by 30.24 (4) and 40.16 (3)° out of the planes of the 3-methyphenyl and 4-methyphenyl rings, respectively. The methyl groups are disordered over two equally occupied positions. In the crystal, inter-molecular N-H⋯O hydrogen bonds link the mol-ecules ...

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ژورنال

عنوان ژورنال: Acta Crystallographica Section E Structure Reports Online

سال: 2012

ISSN: 1600-5368

DOI: 10.1107/s1600536812017795